The best replacement for xrf is xrd.

The best alternatives to xrf are rated as following:
★★★★★  xrd
★★★★★  icp
★★★★★  eds
★★  xbee
★★  icp-ms
★★  aas
★  fire assay
★  libs
★  edx
  txrf
  icp ms
  oes

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Google Trends

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xrf
xrd
icp