The best replacement for nmr is mri.

The best alternatives to nmr are rated as following:
★★★★★  mri
★★★★  ir
★★  vap
★★  epr
★★  mass spec
★★  x-ray crystallography
★  vap test
★  crystallography
  x ray crystallography
  gc-ms
  ftir
  infrared spectroscopy
  carbon 13 nmr
  2d nmr
  hplc
  solid state nmr
  ir spectroscopy

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